顺-1,2-双(二苯基膦)乙烯合成路线 （共 7 条）
反应条件
potassium hydroxide; tetrabutylammomium bromide in tetrahydrofuran T=66°C; 3 h;
参考文献
Russian Journal of General Chemistry, , vol. 64, # 8.1 p. 1134 - 1138
Zhurnal Obshchei Khimii, , vol. 64, # 8 p. 1260 - 1265
反应条件
hydrogen; (tolane)(trimethylphosphane)titanocene P=760 Torr; Ambient temperature;
参考文献
Journal of Organometallic Chemistry, , vol. 287, p. C35 - C38
反应条件
1: triphenylphosphine With lithium in tetrahydrofuran 2: cis-1,2-dichloroethylene in tetrahydrofuran; benzene
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 179, # 7 p. 1251 - 1266
反应条件
in chloroform dissolving cis-bisphosphine in CHCl3, addn. of solid CuCl, stirring for 1 h under steady stream of N2, reduction of volume by rotary evapn., pptn. by cooling to 3°C;; recrystn. from aq. methanol; elem. anal.;
参考文献
Berners-Price, Susan J.; Johnson, Randall K.; Mirabelli, Christopher K.; Faucette, Leo F.; McCabe, Francis L.; Sadler, Peter J.
Inorganic Chemistry, 1987 , vol. 26, p. 3383 - 3387
反应条件
in toluene Kinetics; reductive elimination between -19 and 10°C;; monitored by (1)H-NMR-, (13)C-NMR- and (31)P-NMR-spectroscopy;;
参考文献
Journal of the American Chemical Society, , vol. 110, # 18 p. 6272 - 6273
反应条件
in toluene Kinetics; reductive elimination between -19 and 10°C;; monitored by (1)H-NMR-, (13)C-NMR- and (31)P-NMR-spectroscopy;;
参考文献
Journal of the American Chemical Society, , vol. 110, # 18 p. 6272 - 6273
反应条件
in toluene Kinetics; reductive elimination between -19 and 10°C;; monitored by (1)H-NMR-, (13)C-NMR- and (31)P-NMR-spectroscopy;;
参考文献
Journal of the American Chemical Society, , vol. 110, # 18 p. 6272 - 6273
