反-1,2-双(二苯基磷基)乙烯合成路线 (共 3 条)
反应条件
triethylamine; NiCl2((PPh3)P)2 in N,N-dimethyl-formamide T=120°C; 7 h;
参考文献
Shulyupin, Mstilsav O.; Chirkov, Evgeniy A.; Kazankova, Marina A.; Beletskaya, Irina P.
Synlett, 2005 , # 4 art. no. G46004ST, p. 658 - 660
反应条件
1: chloro-diphenylphosphine With potassium in 1,4-dioxane 10 h; Heating; 2: trans-1,2-dichloroethylene in 1,4-dioxane T=20°C; 10 h; Further stages.;
参考文献
Brunner, Henri; Muschiol, Manfred; Zabel, Manfred
Synthesis, 2008 , # 3 p. 405 - 408
反应条件
potassium tert-butylate in toluene 24 h; Heating;
参考文献
Schmidbaur, Hubert; Paschalidis, Christos; Reber, Gabriele; Mueller, Gerhard
Chemische Berichte, 1988 , vol. 121, p. 1241 - 1246