反应条件
1: 98 percent / sodium azide, 20percent oleum / 1,2-dichloro-ethane / 5 h / 5 - 23 °C
2: 99 percent / 48 h / Heating
3: 90percent nitric acid, conc. H2SO4 / 2 h / 35 - 55 °C
4: HCl(gas) / methanol
View Scheme
参考文献
Nielsen, Arnold T.; DeFusco, Albert A.; Browne, Thomas E.
Journal of Organic Chemistry, 1985 , vol. 50, # 22 p. 4211 - 4218
