1-(4,6-二甲基-3-吡啶基)甲胺合成路线 （共 9 条）
反应条件
hydrogenchloride; palladium on activated charcoal
P=1029.7 Torr; Hydrogenation;
参考文献
Mariella; Leech
Journal of the American Chemical Society, 1949 , vol. 71, p. 331
反应条件
hydrazine; nickel in ethanol; water
T=20°C; Product distribution / selectivity;
参考文献
Coats, Steven J.; Dyatkin, Alexey B.; He, Wei; Lisko, Joseph; Miskowski, Tamara; Ralbovsky, Janet L.; Schulz, Mark
Patent: US2008/269225 A1, 2008 ;
Location in patent: Page/Page column 29 ;
US 20080269225 A1
反应条件
hydrogenchloride; palladium on activated charcoal
P=2206.5 Torr; Hydrogenation;
参考文献
Mariella; Belcher
Journal of the American Chemical Society, 1952 , vol. 74, p. 4049
反应条件
hydrogen; nickel in ethanol
T=130°C; P=152000 Torr;
参考文献
Zubarev; Zav'yalova; Litvinov
Russian Chemical Bulletin, 2005 , vol. 54, # 11 p. 2578 - 2581
反应条件
1: PCl5
2: palladium/charcoal; aq.-ethanolic HCl / 1029.7 Torr / Hydrogenation
View Scheme
参考文献
Mariella; Leech
Journal of the American Chemical Society, 1949 , vol. 71, p. 331
反应条件
1: chlorobenzene; PCl5
2: palladium/charcoal; aq.-ethanolic HCl / 2206.5 Torr / Hydrogenation
View Scheme
参考文献
Mariella; Belcher
Journal of the American Chemical Society, 1952 , vol. 74, p. 4049
反应条件
1: ethanol; piperidine
2: chlorobenzene; PCl5
3: palladium/charcoal; aq.-ethanolic HCl / 2206.5 Torr / Hydrogenation
View Scheme
参考文献
Mariella; Belcher
Journal of the American Chemical Society, 1952 , vol. 74, p. 4049
参考文献
Japan Tobacco Inc.
Patent: US2007/32529 A1, 2007 ;
US 20070032529 A1
反应条件
nickel in methanol
5 h; Heating;
参考文献
Zubarev; Zav'yalova; Litvinov
Russian Chemical Bulletin, 2005 , vol. 54, # 11 p. 2578 - 2581
