氧代[2,3,5,6-四氟-4-(三氟甲基)苯基][2,3,5,6-四氟-4-(三氟甲基)苯基]亚氨基铵合成路线 （共 6 条）
反应条件
dihydrogen peroxide in acetic acid
T=20°C; 50 h;
参考文献
Korobeinicheva, I. K.; Fugaeva, O. M.; Furin, G. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, p. 1391 - 1397
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 7 p. 1537 - 1544
反应条件
ammonium chloride; zinc in ethanol; water
T=50 - 60°C;
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
反应条件
phosphorus trichoride in dichloromethane
T=20°C; 20 h;
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
反应条件
1: zinc powder, NH4Cl / H2O; ethanol / 50 - 60 °C
2: PCl3 / CH2Cl2 / 20 h / 20 °C
View Scheme
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
反应条件
2,3,4,5,6-pentafluorobenzaldehyde
T=100°C; 5 h;
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
反应条件
phosphorus trichoride in dichloromethane
T=20°C; 20 h; further reagents; Product distribution;
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
