2-氯甲基-(6ci,9ci)-4H-3,1-苯并噁嗪-4-酮合成路线 （共 4 条）
反应条件
acetic anhydride
Reflux;
参考文献
Huang, Hui; Gao, Jian-Fang; Cao, Ling-Hua; Wang, Duo-Zhi; Zhang, Jian-Bin; Zhou, Shu-Bao; Zhou, Yu-Qiang
Journal of the Chinese Chemical Society, 2009 , vol. 56, # 2 p. 419 - 424
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 2 h; Product distribution / selectivity;
参考文献
WHITEHEAD INSTITUTE FOR BIOMEDICAL RESEARCH; THE TRUSTEES OF COLUMBIA UNIVERSITY IN THE CITY OF NEW YORK
Patent: WO2006/81337 A2, 2006 ;
Location in patent: Page/Page column 127 ;
反应条件
1: 97 percent / benzene / 2 h / Heating
2: 88 percent / acetic anhydride / 0.67 h / Heating
View Scheme
参考文献
Fetter, Jozsef; Czuppon, Tibor; Hornyak, Gyula; Feller, Antal
Tetrahedron, 1991 , vol. 47, # 45 p. 9393 - 9410
反应条件
in benzene
T=20°C; Reflux;
参考文献
Huang, Hui; Gao, Jian-Fang; Cao, Ling-Hua; Wang, Duo-Zhi; Zhang, Jian-Bin; Zhou, Shu-Bao; Zhou, Yu-Qiang
Journal of the Chinese Chemical Society, 2009 , vol. 56, # 2 p. 419 - 424
