N-(2-氟苯基)甲磺酰胺合成路线 (共 9 条)
反应条件
pyridine in dichloromethane 1) 1 h, 0 deg C; 2) 1 h, 25 deg C;
参考文献
Journal of Organic Chemistry, , vol. 49, # 2 p. 249 - 254
反应条件
copper(I) oxide; caesium carbonate in water T=130°C; 24 h; Sealed tube;
参考文献
Tan, Bryan Yong-Hao; Teo, Yong-Chua; Seow, Ai-Hua
European Journal of Organic Chemistry, 2014 , vol. 2014, # 7 p. 1541 - 1546
反应条件
titanium tetrachloride in chlorobenzene T=132°C; Product distribution;
参考文献
Sundberg, Richard J.; Laurino, Joseph P.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 249 - 254
反应条件
trifluoromethyl hypofluorite in trifluoroacetic acid
参考文献
Journal of Organic Chemistry, , vol. 50, # 23 p. 4576 - 4582
反应条件
titanium tetrachloride in toluene T=110°C;
参考文献
Journal of Organic Chemistry, , vol. 49, # 2 p. 249 - 254
反应条件
1: pyridine / 12 h / 23 °C 2: NaOH / H2O; tetrahydrofuran / 1 h / 23 °C View Scheme
参考文献
Tetrahedron, , vol. 56, # 32 p. 5843 - 5856
反应条件
pyridine T=23°C; Substitution; 12 h;
参考文献
Tetrahedron, , vol. 56, # 32 p. 5843 - 5856
参考文献
Occidental Chemical Corporation
Patent: US4766243 A1, 1988 ;
反应条件
sodium hydride in N,N-dimethyl-formamide
T=110°C;
参考文献
Sundberg, Richard J.; Laurino, Joseph P.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 249 - 254