4’-硝基-[1,1’-联苯]-4-甲醛合成路线 (共 11 条)
反应条件
palladium diacetate; 4-Ph2P-C6H4-2-N-glucosamine; sodium carbonate in tetrahydrofuran; ethanol; water T=60°C; 1 h;
参考文献
Kolodziuk, Robert; Penciu, Alexandra; Tollabi, Mustapha; Framery, Eric; Goux-Henry, Catherine; Iourtchenko, Alexander; Sinou, Denis
Journal of Organometallic Chemistry, 2003 , vol. 687, # 2 p. 384 - 391
反应条件
potassium carbonate in ethanol; water T=50°C; Suzuki-Miyaura Coupling; 19 h; Reagent/catalyst;
参考文献
Pavia, Cinzia; Ballerini, Eleonora; Bivona, Lucia Anna; Giacalone, Francesco; Aprile, Carmela; Vaccaro, Luigi; Gruttadauria, Michelangelo
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2007 - 2018
反应条件
glucosamine-based dicyclohexylarylphosphine; sodium carbonate; palladium diacetate in ethanol; water; toluene T=80°C; Suzuki-Miyaura cross coupling reaction;
参考文献
Konovets, Anzhelika; Penciu, Alexandra; Framery, Eric; Percina, Nathalie; Goux-Henry, Catherine; Sinou, Denis
Tetrahedron Letters, 2005 , vol. 46, # 18 p. 3205 - 3208
反应条件
sodium carbonate; palladium on activated charcoal in ethanol; water T=20°C; Suzuki-Miyaura cross-coupling; 4 h;
参考文献
Kitamura, Yoshiaki; Sakurai, Ai; Udzu, Takahiro; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 43 p. 10596 - 10602
反应条件
1 Pd/C in methanol T=50°C; Suzuki-Miyaura reaction; 0.166667 h; Inert atmosphere;
参考文献
Bonin, Helene; Delbrayelle, Dominique; Demonchaux, Patrice; Gras, Emmanuel
Chemical Communications, 2010 , vol. 46, # 15 p. 2677 - 2679
反应条件
sulfuric acid; potassium nitrate T=-5 - 0°C; 2 h;
参考文献
Link, P. A. J.; Plas, H. C. van der; Mueller, F.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 841 - 848
反应条件
diisobutylaluminium hydride in methanol; water; toluene
反应条件
4-nitro-phenol; α,α-diphenylprolinol O-TMS ether in chloroform T=20°C; 72 h; regioselective reaction;
参考文献
Song, Xixi; Zhang, Xinshuai; Zhang, Shilei; Li, Hao; Wang, Wei
Chemistry - A European Journal, 2012 , vol. 18, # 32 p. 9770 - 9774
反应条件
potassium carbonate in ethanol; water T=50°C; Suzuki coupling; 6 h;
参考文献
European Journal of Organic Chemistry, , # 13 p. 2635 - 2642
反应条件
tetrachloromethane; chromium oxychloride
参考文献
Journal of the Chemical Society, , p. 114