5-甲基-1-苯基-1H-吡唑-4-甲醛合成路线 （共 5 条）
反应条件
4-methylmorpholine N-oxide; tetrapropylammonium perruthennate in dichloromethane 0.666667 h; Molecular sieve;
参考文献
GLAXO GROUP LIMITED
Patent: WO2006/67462 A1, 2006 ;
Location in patent: Page/Page column 47 ;
WO 2006/067462 A1
参考文献
Liebigs Annalen der Chemie, , # 7 p. 1377 - 1388
反应条件
1.1: 2 h / 120 °C 1.2: 2.5 h / 80 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C / Cooling with ice 3.1: manganese(IV) oxide / tetrahydrofuran / 3 h / 70 °C View Scheme
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C / Cooling with ice 2: manganese(IV) oxide / tetrahydrofuran / 3 h / 70 °C View Scheme
反应条件
in xylene 36 h; Heating;
参考文献
Liebigs Annalen der Chemie, , # 7 p. 1377 - 1388
