(1S)-1-(2R)-环氧乙基-2-苯乙基氨基甲酸叔丁酯合成路线 （共 74 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in chloroform Heating;
参考文献
Tetrahedron Letters, , vol. 38, # 19 p. 3483 - 3486
反应条件
potassium carbonate in methanol
反应条件
sodium hydroxide in water
反应条件
1: With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 0.666667 h; 2: With potassium hydroxide in methanol T=20°C; 2 h; Further stages.;
参考文献
Organic letters, , vol. 3, # 15 p. 2349 - 2351
反应条件
1: With potassium hydroxide in ethanol T=0 - 20°C; 1.33333 h; 2: With water in ethanol
参考文献
WO2006/10094 A1, ;
Page/Page column 128-129 ;
WO 2006/010094 A1
反应条件
1: H2 / Pd/C / ethyl acetate / 20 °C 2: Ph3P; diisopropyl azodicarboxylate / CHCl3 / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 13 p. 5075 - 5083
反应条件
potassium hydroxide in ethanol 1 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 31 p. 5453 - 5456
反应条件
1: With formic acid; triethylamine; (pentamethylcyclopentadienyl)RhCl[(S,S)-Tsdpen] in isopropyl alcohol T=25°C; 2: With sodium hydroxide in isopropyl alcohol T=0°C; 3: With water
参考文献
Journal of Organic Chemistry, , vol. 69, # 21 p. 7391 - 7394
反应条件
potassium carbonate in methanol T=0 - 20°C;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 19 p. 2226 - 2229
反应条件
1.1: isobutyl chloroformate; NMM / -15 °C 1.3: 73 percent / HBr 2.1: 62 percent / LiAl(O-t-Bu)3H / ethanol / -78 °C 3.1: KOH / ethanol View Scheme
参考文献
Chemistry Letters, , vol. 36, # 5 p. 648 - 649
