(1S)-1-(2R)-环氧乙基-2-苯乙基氨基甲酸叔丁酯合成路线 （共 74 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 20 h; Heatingvarious temperatures and concentrations of MCPBA; Product distribution;
参考文献
Tetrahedron Letters, , vol. 35, # 28 p. 4939 - 4942
反应条件
sodium tetrahydroborate
参考文献
Tetrahedron Asymmetry, , vol. 6, # 9 p. 2245 - 2247
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Molecular Pharmacology, , vol. 71, # 2 p. 588 - 601
反应条件
1: LDA / tetrahydrofuran / 0.5 h / -78 °C 2: 7.8 g / NaBH4 / toluene; ethanol / 8 h / -78 - 0 °C 3: 89 percent / KOH / ethanol / 2 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 21 p. 7344 - 7347
反应条件
1: 75 percent / CuBr*Me2S / toluene; tetrahydrofuran / -78 - -20 °C 2: Bu4NF / tetrahydrofuran View Scheme
参考文献
Organic letters, , vol. 3, # 15 p. 2349 - 2351
反应条件
1: 100 percent / NaH / tetrahydrofuran / 5 h / 0 °C 2: 75 percent / CuBr*Me2S / toluene; tetrahydrofuran / -78 - -20 °C 3: Bu4NF / tetrahydrofuran View Scheme
参考文献
Organic letters, , vol. 3, # 15 p. 2349 - 2351
反应条件
1: 74 percent / HBr 2: 47 percent / NaBH4 View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 6, # 9 p. 2245 - 2247
反应条件
2: 74 percent / HBr 3: 47 percent / NaBH4 View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 6, # 9 p. 2245 - 2247
反应条件
in hexane T=5 - 45°C; 1 h; Reagent/catalystTemperatureTime;
参考文献
Organic Process Research and Development, , vol. 15, # 2 p. 331 - 338
反应条件
1: With toluene-4-sulfonic acid 2: With potassium hydroxide in methanol Further stages.;
参考文献
Organic letters, , vol. 3, # 15 p. 2349 - 2351
