(2RS,3RS)-3-(2-乙氧基苯氧基)-3-苯基丙烯-1,2-环氧化物合成路线 （共 4 条）
反应条件
1: methanol; ammonia / isopropyl alcohol 2: carbonic acid dimethyl ester / ethanol 3: potassium tert-butylate / isopropyl alcohol; tert-butyl alcohol 4: methanesulfonic acid / acetone View Scheme
参考文献
Henegar, Kevin E.; Ball, Cynthia T.; Horvath, Carolyn M.; Maisto, Keith D.; Mancini, Sarah E.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 346 - 353
反应条件
1: 32percent NH4OH / methanol / 6 h / sealed flask 2: 98 percent / Et3N / CH2Cl2 / 0.5 h / -10 - -5 °C 3: 86 percent / t-BuOK / 2-methyl-propan-2-ol / 3 h / Ambient temperature 4: RED-AL / toluene / 4 h / Ambient temperature View Scheme
参考文献
Henegar, Kevin E.; Ball, Cynthia T.; Horvath, Carolyn M.; Maisto, Keith D.; Mancini, Sarah E.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 346 - 353
反应条件
1: 32percent NH4OH / methanol / 6 h / sealed flask
2: ethyl acetate / 16 h
View Scheme
参考文献
Henegar, Kevin E.; Ball, Cynthia T.; Horvath, Carolyn M.; Maisto, Keith D.; Mancini, Sarah E.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 346 - 353
反应条件
methanol; ammonia in isopropyl alcohol
参考文献
Assaf, Georges; Checksfield, Graham; Critcher, Doug; Dunn, Peter J.; Field, Stuart; Harris, Laurence J.; Howard, Roger M.; Scotney, Gemma; Scott, Adam; Mathew, Suju; Walker, Geoffrey M. H.; Wilder, Alexander
Green Chemistry, 2012 , vol. 14, # 1 p. 123 - 129
