thionyl chloride; triethylamine in tetrachloromethane
T=0°C; 0.0166667 h;
参考文献
Blatcher, Philip; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1055 - 1066
in dichloromethane
T=-78°C; Addition; Desilylation;
参考文献
Aggarwal, Varinder K.; Eames, Jason; Villa, Maria-Jesus; McIntyre, Sara; Sansbury, Francis H.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 2000 , # 4 p. 532 - 546
1: 73 percent / Et3N / dimethylformamide / 12 h / 80 °C
2: 93 percent / CH2Cl2 / -78 °C
View Scheme
参考文献
Aggarwal, Varinder K.; Eames, Jason; Villa, Maria-Jesus; McIntyre, Sara; Sansbury, Francis H.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 2000 , # 4 p. 532 - 546
