(2RS,3RS)-3-(2-乙氧基苯氧基)-2-甲烷磺酰基氧基-1-(4-硝基苯甲酰氧基)-3-苯基丙烷合成路线 (共 3 条)
反应条件
With triethylamine in dichloromethane T=0 - 5°C; 0.5 h;
参考文献
Melloni; Della Torre; Lazzari; et al. Tetrahedron, 1985 , vol. 41, # 7 p. 1393 - 1399
反应条件
Multi-step reaction with 2 steps 1: 61 percent / pyridine / 2 h / -10 °C2: 84 percent / Et3N / CH2Cl2 / 0.5 h / 0 - 5 °C
参考文献
Melloni; Della Torre; Lazzari; et al. Tetrahedron, 1985 , vol. 41, # 7 p. 1393 - 1399
反应条件
Multi-step reaction with 4 steps 1: MCPBA / CH2Cl2 / 0 deg C, 1.5 h, then RT, 24 h2: 1.) NaOH / 1.) H2O, 70 deg C; 2.) H2O, 70 deg C, 2.5 h3: 61 percent / pyridine / 2 h / -10 °C4: 84 percent / Et3N / CH2Cl2 / 0.5 h / 0 - 5 °C
参考文献
Melloni; Della Torre; Lazzari; et al. Tetrahedron, 1985 , vol. 41, # 7 p. 1393 - 1399