(1R,2S)-(-)-反-2-苯基-1-环己醇合成路线 (共 53 条)
反应条件
sulfuric acid in tetrahydrofuran 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 58, # 16 p. 4484 - 4486
反应条件
phosphate buffer in diethyl ether 240 h; Ambient temperaturechicken liver acetone powder (CLAP);
参考文献
Basavaiah, Deevi; Krishna, Peddinti Rama
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 1 p. 131 - 134
反应条件
sodium tetrahydroborate; nickel dichloride in ethanol
参考文献
Denmark, Scott E.; Dixon, Julie A.
Journal of Organic Chemistry, 1997 , vol. 62, # 21 p. 7086 - 7087
反应条件
platinum(IV) oxide; hydrogen; acetic acid T=60°C; P=15001.5 Torr; 4 h; Autoclave; optical yield given as percent de;
参考文献
Sukhorukov, Alexey Yu.; Boyko, Yaroslav D.; Nelyubina, Yulia V.; Gerard, Stephane; Ioffe, Sema L.; Tartakovsky, Vladimir A.
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5465 - 5469
反应条件
(S,S)(4-JandaJel-CH2-O(CH2)3O)-2(BnN(Me)CH2)N(Me)pyrrolidine; 4 A molecular sieve; triethylamine in dichloromethane T=-78°C; 11 h;
参考文献
Clapham; Cho; Janda
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 868 - 873
反应条件
1: With hydrogen in methanol T=70 - 75°C; P=30003 Torr; 5.5 h; Autoclave; 2: With dimethyl sulfoxide 0.5 h; RefluxInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 46 p. 8082 - 8091
反应条件
nickel in ethanol 2 h; Heating;
参考文献
King, S. Bruce; Sharpless, K. Barry
Tetrahedron Letters, 1994 , vol. 35, # 31 p. 5611 - 5612
参考文献
Tetrahedron Asymmetry, , vol. 5, # 2 p. 223 - 234
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Reduction;
参考文献
European Journal of Organic Chemistry, , # 21 p. 3595 - 3600
反应条件
potassium carbonate 23 h; Ambient temperature;
参考文献
Carpenter, Bryon E.; Hunt, Ian R.; Keay, Brian A.
Tetrahedron Asymmetry, 1996 , vol. 7, # 11 p. 3107 - 3108