N-Fmoc-N’-(4-甲氧基-2,3,6-三甲基苯磺酰基)-L-精氨酸合成路线 (共 3 条)
反应条件
N-ethyl-N,N-diisopropylamine in chloroform
参考文献
Atherton, Eric; Sheppard, Robert C.; Wade, John D.
Journal of the Chemical Society, Chemical Communications, 1983 , # 19 p. 1060 - 1062
反应条件
trifluoroacetic acid in water kinetics of acidolytic removal of Mtr protecting group; other solvents;
参考文献
Ali, Syed Safdar; Echner, Hartmut; Khan, Khalid Mohammed; Schroeder, Christoph; Hasan, Mashooda; et al.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1994 , vol. 49, # 10 p. 1425 - 1433
反应条件
Solid phase synthesis; the next amino acids are: Fmoc-Gly-OOBt, Fmoc-Tyr-OOBt, Fmoc-Ser-OOBt, Fmoc-Trp-OOBt, Fmoc-His(Trt)-OBT, pGlu-OOBt; Yield given. Multistep reaction;
参考文献
Breipohl, G.; Knolle, J.; Stueber, W.
Tetrahedron Letters, 1987 , vol. 28, # 46 p. 5651 - 5654