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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
98952-64-8
合成路线
（共 13 条）
98952-64-8
+
693-02-7
1-己炔
→
反应条件
104919-72-4
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide 12 h; Heating;
参考文献
Yasuhara, Akito; Kanamori, Yuichi; Kaneko, Masashi; Numata, Atsushi; Kondo, Yoshinori; Sakamoto, Takao
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 4 p. 529 - 534
98952-64-8
→
反应条件
934-34-9
2-羟基苯并噻唑
反应条件
1: With copper(l) iodide; Na2S*9H2O in N,N-dimethyl-formamide T=80°C; 12 h; Inert atmosphere; 2: With acetic acid in N,N-dimethyl-formamide T=130°C; 36 h; Inert atmosphere;
参考文献
Li, Jiaojiao; Zhang, Yihua; Jiang, Yongwen; Ma, Dawei
Tetrahedron Letters, 2012 , vol. 53, # 20 p. 2511 - 2513
98952-64-8
→
反应条件
87-51-4
吲哚-3-乙酸
反应条件
1: palladium(II) acetate; diisopropylethylamine; butyltriethylammonium chloride / dimethylformamide / 6 h / 80 °C 2: trifluoroacetic acid / CH2Cl2 / 1.5 h / 20 °C 3: KOH / methanol / Heating View Scheme
参考文献
Taniguchi, Takahiko; Nagata, Hiroshi; Kanada, Regina Mikie; Kadota, Kohei; Takeuchi, Miwako; Ogasawara, Kunio
Heterocycles, 2000 , vol. 52, # 1 p. 67 - 71
64-17-5
乙醇
+
1942-45-6
4-辛炔
+
201230-82-2
+
98952-64-8
→
反应条件
87-25-2
2-氨基苯甲酸乙酯
反应条件
1: octyne-4; carbon monoxide; N-(ethoxycarbonyl)-2-iodoaniline With pyridine; palladium diacetate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=100°C; P=760 Torr; 12 h; 2: ethanol With sodium hydroxide T=20°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6772 - 6780
64-17-5
乙醇
+
999-78-0
4,4-二甲基-2-戊炔
+
201230-82-2
+
98952-64-8
→
反应条件
87-25-2
2-氨基苯甲酸乙酯
反应条件
1: 4,4-dimethyl-2-pentyne; carbon monoxide; N-(ethoxycarbonyl)-2-iodoaniline With pyridine; palladium diacetate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=100°C; P=760 Torr; 12 h; 2: ethanol With sodium hydroxide T=20°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6772 - 6780
64-17-5
乙醇
+
201230-82-2
+
4250-82-2
(3,3-二甲基-1-丁炔)-苯
+
98952-64-8
→
反应条件
87-25-2
2-氨基苯甲酸乙酯
反应条件
1: carbon monoxide; phenyl-tert-butylacetylene; N-(ethoxycarbonyl)-2-iodoaniline With pyridine; palladium diacetate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=100°C; P=760 Torr; 12 h; 2: ethanol With sodium hydroxide T=20°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6772 - 6780
1942-45-6
4-辛炔
+
201230-82-2
+
98952-64-8
→
反应条件
118-48-9
靛红酸酐
反应条件
pyridine; palladium diacetate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=100°C; P=760 Torr; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6772 - 6780
201230-82-2
+
1504-58-1
3-苯基-2-丙炔-1-醇
+
98952-64-8
→
反应条件
138712-65-9
反应条件
1: With pyridine; palladium diacetate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=100°C; P=760 Torr; 12 h; 2: With sodium hydroxide in ethanol T=20°C; 0.5 h;
参考文献
Kadnikov, Dmitry V.; Larock, Richard C.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6772 - 6780
615-43-0
2-碘苯胺
+
541-41-3
氯甲酸乙酯
→
反应条件
98952-64-8
反应条件
potassium carbonate in acetone T=20°C; 3 h;
参考文献
Kadnikov, Dmitry V.; Larock, Richard C.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6772 - 6780
64-17-5
乙醇
+
1202047-19-5
→
反应条件
98952-64-8
反应条件
1: 1-tert-butyl-1-isopropyl-3-phenylurea With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane T=0°C; 3 h; Inert atmosphere; 2: ethanol With iodine in tetrahydrofuran; diethyl ether; hexane T=-78°C; Inert atmosphere;
参考文献
Houlden, Chris E.; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Organic Letters, 2010 , vol. 12, # 13 p. 3090 - 3092
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