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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
间氯苯乙酮
合成路线
（共 137 条）
99-02-5
间氯苯乙酮
→
反应条件
36640-43-4
3-(3-氯苯基)-1-苯基-1H-吡唑-4-甲醛
反应条件
1.1: acetic acid; sodium hydroxide / ethanol / 1 h / Reflux 2.1: trichlorophosphate / 0.5 h / 0 - 5 °C 2.2: 3 h / 50 °C View Scheme
参考文献
Thakrar, Shailesh; Bavishi, Abhay; Bhavsar, Dhairya; Parekh, Shrey; Vala, Hardev; Radadiya, Ashish; Parmar, Manisha; Savant, Mahesh; Shah, Anamik
Synthetic Communications, 2012 , vol. 42, # 22 p. 3269 - 3278
1779-49-3
甲基三苯基溴化膦
+
99-02-5
间氯苯乙酮
→
反应条件
1712-71-6
3-异丙烯基氯代苯
反应条件
1: Methyltriphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran T=0°C; 0.75 h; Inert atmosphere; 2: methyl (3-chlorophenyl)-ketone in tetrahydrofuran T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Tripathi, Chandra Bhushan; Mukherjee, Santanu
Angewandte Chemie - International Edition, 2013 , vol. 52, # 32 p. 8450 - 8453
Angew. Chem., 2013 , vol. 125, # 32 p. 8608 - 8611,4
99-02-5
间氯苯乙酮
→
反应条件
117538-45-1
2-溴-1-(3-氯苯基)乙醇
反应条件
1: Br2 / benzene / 1 h 2: 100 percent / NaBH4 / ethanol / 0 °C View Scheme
参考文献
Perrone, Roberto; Berardi, Francesco; Leopoldo, Marcello; Tortorella, Vincenzo; Lograno, Marcello D.; et al.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 16 p. 3045 - 3049
99-02-5
间氯苯乙酮
→
反应条件
648425-33-6
反应条件
1.1: sodium hydride / toluene / 0.5 h / 4 °C 1.2: 77 percent / toluene / 4 - 20 °C 2.1: 92 percent / diisobutylaluminum hydride / toluene / 1 h / -5 - 20 °C 3.1: 76 percent / methanesulfonyl chloride; Et3N / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Pinna, Gerard Aime; Cignarella, Giorgio; Ruiu, Stefania; Loriga, Giovanni; Murineddu, Gabriele; Villa, Stefania; Grella, Giuseppe Enrico; Cossu, Gregorio; Fratta, Walter
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4015 - 4026
99-02-5
间氯苯乙酮
→
反应条件
648425-38-1
反应条件
1.1: sodium hydride / toluene / 0.5 h / 4 °C 1.2: 77 percent / toluene / 4 - 20 °C 2.1: 92 percent / diisobutylaluminum hydride / toluene / 1 h / -5 - 20 °C View Scheme
参考文献
Pinna, Gerard Aime; Cignarella, Giorgio; Ruiu, Stefania; Loriga, Giovanni; Murineddu, Gabriele; Villa, Stefania; Grella, Giuseppe Enrico; Cossu, Gregorio; Fratta, Walter
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4015 - 4026
867-13-0
膦酰乙酸三乙酯
+
99-02-5
间氯苯乙酮
→
反应条件
反应条件
1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in toluene T=4°C; 0.5 h; 2: methyl (3-chlorophenyl)-ketone in toluene T=4 - 20°C; Horner-Emmons condensation;
参考文献
Pinna, Gerard Aime; Cignarella, Giorgio; Ruiu, Stefania; Loriga, Giovanni; Murineddu, Gabriele; Villa, Stefania; Grella, Giuseppe Enrico; Cossu, Gregorio; Fratta, Walter
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4015 - 4026
867-13-0
膦酰乙酸三乙酯
+
99-02-5
间氯苯乙酮
→
反应条件
648425-41-6
反应条件
1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in tetrahydrofuran; mineral oil T=0 - 20°C; Inert atmosphere; 2: methyl (3-chlorophenyl)-ketone in tetrahydrofuran; mineral oil T=20°C; Inert atmosphere;
参考文献
Shang, Jian; Han, Zhaobin; Li, Yang; Wang, Zheng; Ding, Kuiling
Chemical Communications, 2012 , vol. 48, # 42 p. 5172 - 5174
99-02-5
间氯苯乙酮
→
反应条件
70424-69-0
2,3,3',4,5-五氯联苯
反应条件
1: hydroquinone, PCl5 2: 1.25 h / 63 - 75 °C 3: KOH / aq. ethanol / 12 h / Heating 4: 80.6 percent / benzene 5: 44.7 percent / cyclohexane / 19 h / Irradiation View Scheme
参考文献
Pyle, James L.; Shaffer, Alan A.; Cantrell, Joseph S.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 115 - 118
67-56-1
甲醇
+
99-02-5
间氯苯乙酮
→
反应条件
73585-53-2
反应条件
hydrogen bromide T=25°C; Rate constant;
参考文献
Toullec, Jean; El-Alaoui, Mohiedine
Journal of Organic Chemistry, 1986 , vol. 51, # 21 p. 4054 - 4061
99-02-5
间氯苯乙酮
→
反应条件
7394-51-6
反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere 1.2: 20 °C / Inert atmosphere 2.1: water; potassium hydroxide / 100 °C / Inert atmosphere View Scheme
参考文献
Shen, Li-Tao; Shao, Pan-Lin; Ye, Song
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1943 - 1948
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