Sienkowska, Monika J.; Farrar, John M.; Zhang, Fan; Kusuma, Sharat; Heiney, Paul A.; Kaszynski, Piotr
Journal of Materials Chemistry, 2007 , vol. 17, # 14 p. 1399 - 1411
1: Potassium carbonate / methanol; H2O / 15 h / Heating
2: conc. sulphuric acid (90percent) / 24 h / 0 - 5 °C
View Scheme
参考文献
Sarkhel, B. K.; Srivastava, Jagdish N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 2 p. 158 - 159
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
1: 84 percent / sodium hydroxide / heating
5: 28.8 g / fluoroboric acid, sodium nitrite / H2O
6: 7.6 g / warming, distillation
7: 1.456 g / boron tribromide / CH2Cl2 / 52 h
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
1: methanol; 3,5-di(hydroxy)benzoic acid With toluene-4-sulfonic acid in hexane
Reflux;
2: chloromethyl methyl ether With potassium carbonate in acetone
Reflux;
