1: 84 percent / sodium hydroxide / heating 5: 28.8 g / fluoroboric acid, sodium nitrite / H2O 6: 7.6 g / warming, distillation 7: 1.) lithium / 1.) ether, 2 h 8: decarboxylation 9: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
1: K2CO3 / acetone / 72 h / Heating 2: NaOH / ethanol / 1.5 h / Heating 3: thionyl chloride / benzene / 1 h / Heating 4: Et3N / diethyl ether / 4 h 5: 86 percent / silver benzoate, Et3N / 1 h / Heating 6: 55 percent / AcOH, perchloric acid (3 drops) / 0.25 h / Ambient temperature 7: NaH / tetrahydrofuran / 2 h / Ambient temperature 8: tetrahydrofuran / 0.5 h 9: 27 percent / ethanol / 1 h / Irradiation 10: 9 percent / KOH (40percent) / ethanol; dioxane / 2.5 h / Heating 11: 65 percent / potassium dichromate / dioxane; acetic acid / 5 h / Ambient temperature 12: 28 percent / MnO2, H2SO4 (conc.) / 0.5 h / 60 °C 13: silver oxide / dioxane / 1.5 h / Ambient temperature View Scheme
参考文献
Katagiri, Nobuya; Nakano, Jun; Kato, Tetsuzo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2710 - 2716
