2,6-二溴-4-硝基苯酚合成路线 (共 54 条)
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide; calcium carbonate in methanol; dichloromethane
参考文献
Kakinami; Suenaga; Yamaguchi; Okamoto; Kajigaeshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3373 - 3375
反应条件
nitric acid in diethyl ether T=20°C; 15 h;
参考文献
Adimurthy, Subbarayappa; Vaghela, Sanjay S.; Vyas, Punita V.; Bhatt, Anjani K.; Ramachandraiah, Gadde; Bedekar, Ashutosh V.
Tetrahedron Letters, 2003 , vol. 44, # 34 p. 6393 - 6395
反应条件
N-bromosuccinmide; lithium perchlorate; silica gel in dichloromethane T=20°C; 0.0833333 h;
参考文献
Canadian Journal of Chemistry, , vol. 83, # 2 p. 146 - 149
反应条件
acetic acid; sodium nitrite T=20°C; 3 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 44, # 5 p. 688 - 692
反应条件
ethanol beim Bromieren;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 205, p. 91,94
参考文献
Chemische Berichte, , vol. 21, p. 3316
Justus Liebigs Annalen der Chemie, , vol. 279, p. 30
Journal of the Chemical Society, , vol. 79, p. 688
反应条件
water; bromine T=100°C;
参考文献
Journal of the Chemical Society, , vol. 51, p. 149
Journal of the Chemical Society, , vol. 28, p. 521
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, , p. 427
反应条件
acetic acid; sodium nitrite T=12 - 15°C;
参考文献
American Chemical Journal, , vol. 43, p. 394
反应条件
nitric acid; acetic acid T=0°C;
参考文献
Journal of the Chemical Society, , vol. 101, p. 1825
反应条件
acetic acid; sodium nitrite T=20°C;
参考文献
Russian Journal of Organic Chemistry, , vol. 44, # 5 p. 688 - 692