3.5-二硝基苯甲酰氯合成路线 （共 144 条）
参考文献
Kleene; Fried
Journal of the American Chemical Society, 1940 , vol. 62, p. 3516
参考文献
Phillips; Keenan
Journal of the American Chemical Society, 1931 , vol. 53, p. 1924,1926
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
16 h; Ambient temperature;
参考文献
Amyes, Tina L.; Richard, John P.
Journal of the American Chemical Society, 1990 , vol. 112, # 26 p. 9507 - 9512
参考文献
Phillips; Keenan
Journal of the American Chemical Society, 1931 , vol. 53, p. 1924,1926
参考文献
Spaeth; Pailer; Schmid
Chemische Berichte, 1941 , vol. 74, p. 1556
反应条件
1: Fischer base
2: POCl3 / dioxane / 4 h / 80 °C
3: aq. NaOH / Ambient temperature
View Scheme
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
4 h; Ambient temperature;
参考文献
Amyes, Tina L.; Richard, John P.; Novak, Michael
Journal of the American Chemical Society, 1992 , vol. 114, # 21 p. 8032 - 8041
反应条件
quinoline; chloroform
参考文献
Reichstein
Helvetica Chimica Acta, 1926 , vol. 9, p. 802
反应条件
1.1: N,N-dimethyl-acetamide / 3 h / 0 - 20 °C
1.2: 90 percent / p-TsOH / N,N-dimethyl-acetamide; p-xylene / 6 h / 160 °C
2.1: 7.5 g / SnCl2*7H2O; aq. HCl / 90 - 100 °C
View Scheme
参考文献
Rtishchev; Nosova; Solovskaya; Romashkova; Kudryavtsev
Russian Journal of General Chemistry, 2005 , vol. 75, # 10 p. 1584 - 1593
反应条件
triethylamine in tetrahydrofuran
Inert atmosphereReflux;
参考文献
Baehring, Steffen; Kim, Dong Sub; Duedal, Troels; Lynch, Vincent M.; Nielsen, Kent A.; Jeppesen, Jan O.; Sessler, Jonathan L.
Chemical Communications, 2014 , vol. 50, # 41 p. 5497 - 5499
