3.5-二硝基苯甲酰氯合成路线 (共 144 条)
反应条件
tetrachloromethane; aluminium trichloride
参考文献
Hill
Journal of the American Chemical Society, 1954 , vol. 76, p. 2329,2330
反应条件
tri-n-butyl-tin hydride; sodium iodide; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in ethylene glycol dimethyl ether T=25°C; 0.25 h;
参考文献
Malanga, Corrado; Mannucci, Serena; Lardicci, Luciano
Tetrahedron Letters, 1997 , vol. 38, # 46 p. 8093 - 8096
反应条件
sulfuric acid; methylmagnesium bromide; acetic acid in tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; chloroform; water
参考文献
Asahi Kasei Kogyo Kabushiki Kaisha
Patent: US6037362 A1, 2000 ;
参考文献
Zentmyer; Wagner
Journal of Organic Chemistry, 1949 , vol. 14, p. 967,969, 977
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Saunders
Journal of the Chemical Society, 1938 , p. 1400
参考文献
El Seoud, Omar A.; Ruasse, Marie-Francoise; Rodrigues, Wagner A.
Journal of the Chemical Society. Perkin Transactions 2, 2002 , # 6 p. 1053 - 1058
参考文献
Ismailskii; Belozwetow
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 650,655
Chem.Abstr., 1942 , p. 436
参考文献
Brown; Kremers
Journal of the American Pharmaceutical Association (1912-1977), vol. 11, p. 608
Chem. Zentralbl., 1923 , vol. 94, # III p. 1358
参考文献
Zippi; Andres; Morimoto; Williams
Synthetic Communications, 1995 , vol. 25, # 17 p. 2685 - 2693
反应条件
1.1: N,N-dimethyl-acetamide / 0 - 20 °C 1.2: p-TsOH / N,N-dimethyl-acetamide; p-xylene / 160 °C 2.1: SnCl2*7H2O; aq. HCl / 90 - 100 °C View Scheme
参考文献
Rtishchev; Nosova; Solovskaya; Romashkova; Kudryavtsev
Russian Journal of General Chemistry, 2005 , vol. 75, # 10 p. 1584 - 1593
反应条件
in chlorobenzene; tert-butyl alcohol T=25°C; other concentration of tert-butyl alcohole; Rate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, # 9 p. 1702 - 1710
Zhurnal Organicheskoi Khimii, , vol. 22, # 9 p. 1896 - 1904