反应条件
1: thionyl chloride / 1 h / 100 °C 2: CH2Cl2 / 14 h / Ambient temperature 3: 70 percent / thionyl chloride / benzene; CH2Cl2 / 1.) reflux, 2.) room temperature, 2.5 h 4: 1.) CuI, 2.) n-butyllithium, 4.) MeOH 5: 1.) 4.5 N HCl / 1.) reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, p. 7178