3,4-二羟基-2'-氯苯乙酮合成路线 (共 71 条)
参考文献
Journal of the Chemical Society, , vol. 105, p. 1051
参考文献
DE71312 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 858
参考文献
Journal of the Chemical Society, , vol. 97, p. 2520
Journal of the Chemical Society, , vol. 105, p. 1051
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 25, p. 154
Chemische Berichte, 26 Ref. <1893>, 58
参考文献
Chemische Berichte, , vol. 59, p. 1069,1070
参考文献
Chemische Berichte, , vol. 61, p. 2605
反应条件
1: 86 percent / CF3COOH, Et3SiH / Ambient temperature 2: 57 percent / K2CO3, NaI / acetone / 15 h / Heating 3: 92 percent / tetrahydrofuran; ethanol; methanol / 12 h / Heating 4: 65 percent / EtSH, BF3*Et2O / 1 h / Ambient temperature View Scheme
参考文献
Chang; Ares; Anderson; Sabol; Wallace; Farooqui; Uretsky; Miller
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 214 - 218
反应条件
1: 77 percent / KOH / methanol / 2 h / Ambient temperature 2: 72 percent / CF3COOH, Et3SiH / CH2Cl2 / 7 h / Ambient temperature 3: 95 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / 0 °C View Scheme
参考文献
Chang; Ares; Anderson; Sabol; Wallace; Farooqui; Uretsky; Miller
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 214 - 218
反应条件
1: 77 percent / KOH / methanol / 2 h / Ambient temperature 2: 72 percent / CF3COOH, Et3SiH / CH2Cl2 / 7 h / Ambient temperature View Scheme
参考文献
Chang; Ares; Anderson; Sabol; Wallace; Farooqui; Uretsky; Miller
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 214 - 218
反应条件
1: 77 percent / KOH / methanol / 2 h / Ambient temperature 2: 72 percent / CF3COOH, Et3SiH / CH2Cl2 / 7 h / Ambient temperature 3: 95 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / 0 °C 4: 90 percent / m-chloroperbenzoic acid / dimethylformamide / Ambient temperature View Scheme
参考文献
Chang; Ares; Anderson; Sabol; Wallace; Farooqui; Uretsky; Miller
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 214 - 218