反应条件
1: 130 mg / aq. perchloric acid / acetonitrile / 4 h / 0 °C 2: 158 mg / sodium hydride / tetrahydrofuran / 4 h / 20 °C 3: 1.) MCPBA, 2.) trimethyl phosphite / 1.) methylene chloride, -78 deg C, 30 min, room temperature, 1 h, 2.) reflux, 8 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, p. 3554