1,2-二氯-4-硝基苯合成路线 （共 148 条）
反应条件
1: N,N-dimethyl-formamide / 20 - 100 °C 2: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C View Scheme
参考文献
WO2011/15037 A1, ;
US2011/212975 A1, ;
反应条件
iodine T=140°C; 6 h;
参考文献
Du, Xiaohua; Zheng, Mei; Chen, Sheng; Xu, Zhenyuan
Synlett, 2006 , # 12 p. 1953 - 1955
反应条件
pyridine; Rhodium trichloride; bis(acetylacetonate)oxovanadium; p-methylnitrobenzene; Azobenzene in chlorobenzene T=175°C; P=60004.8 Torr; 1 h; other reagents; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 546 - 549
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 606 - 610
反应条件
Pd(dippp)2 in benzene T=90°C; Methylation; 22 h;
参考文献
Synthesis, , # 4 p. 571 - 575
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=90°C; Methylation; 22 h;
参考文献
Synthesis, , # 4 p. 571 - 575
反应条件
ammonium acetate; acetic acid
参考文献
Kiprianow; Daschewskii
Ukrainskii Khimicheskii Zhurnal (Russian Edition), 1930 , vol. 5, p. Nauk.tech.Cast.S.241,247
Chem.Abstr., 1931 , p. II 426
Full Text Show Details
Dow Chem.Co.
Patent: US1882811 , 1929 ;
参考文献
Perna
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1903 , vol. 35, p. 114
Chem. Zentralbl., 1903 , vol. 74, # I p. 1127
Full Text Show Details
Beilstein; Kurbatow
Justus Liebigs Annalen der Chemie, 1876 , vol. 182, p. 108
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1877 , vol. 9, p. 110
反应条件
in N,N-dimethyl-formamide T=20 - 100°C;
参考文献
The University of Hong Kong
Patent: US2011/212975 A1, 2011 ;
Location in patent: Page/Page column 13; 18 ;
参考文献
Pfizer Inc.
Patent: US4797401 A1, 1989 ;
反应条件
ammonium formate; zinc in acetonitrile T=25 - 30°C; 1 h; sonification;
参考文献
Shi, Qi Xun; Lu, Rong Wen; Jin, Kun; Zhang, Zhu Xia; Zhao, De Feng
Chemistry Letters, 2006 , vol. 35, # 2 p. 226 - 227
