1,2-二氯-4-硝基苯合成路线 (共 148 条)
反应条件
bei der Chlorierung;
参考文献
Cohen; Bennett
Journal of the Chemical Society, 1905 , vol. 87, p. 324
反应条件
triethylamine in N,N-dimethyl-formamide 2 h; Heating;
参考文献
Xu, Zhenyuan; Du, Xiaohua; Gu, Jianbo
Organic Preparations and Procedures International, 2003 , vol. 35, # 4 p. 439 - 443
反应条件
1: K2CO3 2: aq. NaOH View Scheme
参考文献
Baker,B.R.; Ashton,W.T.
Journal of Medicinal Chemistry, 1970 , vol. 13, p. 1165 - 1170
反应条件
bei der Chlorierung;
参考文献
Cohen; Bennett
Journal of the Chemical Society, 1905 , vol. 87, p. 324
反应条件
potassium carbonate in xylenes 72 h; Heating / reflux;
参考文献
Schering-Plough Animal Health Corporation
Patent: US2006/281695 A1, 2006 ;
Location in patent: Page/Page column 38 ;
反应条件
1: alcohol; ammonia 2: durch Bromierung View Scheme
参考文献
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1913 , vol. <5> 22 I, p. 823
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1914 , vol. <5> 23 I, p. 283 Anm.
反应条件
hydrogen in ethanol; water T=25°C; P=760.051 Torr; 3 h; Autoclave;
参考文献
Fan, Guang-Yin; Zhang, Lei; Fu, Hai-Yan; Yuan, Mao-Lin; Li, Rui-Xiang; Chen, Hua; Li, Xian-Jun
Catalysis Communications, 2010 , vol. 11, # 5 p. 451 - 455
反应条件
hydrogen; sodium hydrogencarbonate; dichloro(1,5-cyclooctadiene)platinum(II); β-cyclodextrin modified diphosphine in water; toluene T=80°C; Reduction; P=15001.2 Torr; 24 h; Title compound not separated from byproducts;
参考文献
Synthesis, , # 9 p. 1555 - 1557
反应条件
1: With carbon monoxide; {Pd([1,10]phenanthroline)2}[BF4]2; triethylamine in tetrahydrofuran T=100°C; P=7500.75 Torr; 6 h; 2: in benzene T=200°C; P=7500.75 Torr; 3 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ragaini, Fabio; Cenini, Sergio; Brignoli, Daniela; Gasperini, Michela; Gallo, Emma
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 460 - 466
反应条件
tri-ruthenium(0)dodecacarbonyl; carbon monoxide T=160°C; P=30002.4 Torr; 6 h; var. ligands, other nitroarenes, other olefines; Product distributionRate constant;
参考文献
Journal of the American Chemical Society, , vol. 118, # 47 p. 11964 - 11965