2-氨基-4-硝基苯甲醚合成路线 （共 59 条）
参考文献
Chem. Zentralbl., , vol. 79, # II p. 1826
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>87, p. 504
参考文献
Journal of the Chemical Society, , vol. 111, p. 232
反应条件
1.1: HCl; NaNO2 / H2O / 0.5 h / 0 - 5 °C 1.2: H2O 2.1: 75 percent / HF; pyridine / 8 h / 12 °C / Irradiation View Scheme
参考文献
Sawaguchi, Masanori; Fukuhara, Tsuyoshi; Yoneda, Norihiko
Journal of Fluorine Chemistry, 1999 , vol. 97, # 1-2 p. 127 - 133
参考文献
Bermudez, Jose; Dabbs, Steven; King, Frank D.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 7 p. 1932 - 1935
参考文献
Emokpae, Thomas A.; Eguavoen, Osa; Khalil-Ur-Rahman; Hirst, Jack
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 832 - 834
反应条件
1: formic acid With acetic anhydride T=0 - 32°C; 1 h; 2: 2-methoxy-5-nitroaniline T=32°C;
参考文献
CLF MEDICAL TECHNOLOGY ACCELERATION PROGRAM, INC.
Patent: WO2006/102642 A1, 2006 ;
Location in patent: Page/Page column 8; 13; 1/6 ;
反应条件
1.1: p-TSA / benzene / 3 h / Heating 2.1: 5 h / 80 °C 3.1: 9.54 g / H2O / 1 h / 100 °C 4.1: K2CO3 / CH2Cl2 / 1 h / 20 °C 5.1: H2 / 5 percent Pd/C / ethyl acetate 6.1: K2CO3 / ethyl acetate / 1 h 7.1: 670 mg / K2CO3; MeOH / 2 h / 0 °C 8.1: NaNO2; H2SO4 8.2: 85 percent / H2SO4 View Scheme
参考文献
Shiozawa, Tatsushi; Tada, Atsuko; Nukaya, Haruo; Watanabe, Tetsushi; Takahashi, Yoshifumi; Asanoma, Masaharu; Ohe, Takeshi; Sawanishi, Hiroyuki; Katsuhara, Taka; Sugimura, Takashi; Wakabayashi, Keiji; Terao, Yoshiyasu
Chemical Research in Toxicology, 2000 , vol. 13, # 7 p. 535 - 540
反应条件
1: Sandmeyer reaction 2: tin(II) chloride, HCl View Scheme
参考文献
Emokpae, Thomas A.; Eguavoen, Osa; Khalil-Ur-Rahman; Hirst, Jack
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 832 - 834
反应条件
tert.-butylhydroperoxide; 3 A molecular sieve; zirconium tetra-t-butoxide in dichloromethane 3.5 h; Ambient temperature;
参考文献
Krohn, Karsten; Kuepke, Jochen; Rieger, Hagen
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 4 p. 335 - 339
