反应条件
1: sodium tetrahydroborate / ethanol / 2 h / 0 - 20 °C / |Inert atmosphere
2: iron; ammonium chloride / water; ethanol / |Inert atmosphere; |Reflux
3: triethylamine / dichloromethane / 16 h / 20 °C / |Inert atmosphere
4: sodium hydroxide / methanol / 2.5 h / 20 °C / |Inert atmosphere
5: Dess-Martin periodane / dichloromethane / 0.33 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Storz, Michael P.; Maurer, Christine K.; Zimmer, Christina; Wagner, Nathalie; Brengel, Christian; De Jong, Johannes C.; Lucas, Simon; Muesken, Mathias; Haeussler, Susanne; Steinbach, Anke; Hartmann, Rolf W.
Journal of the American Chemical Society, 2012 , vol. 134, # 39 p. 16143 - 16146