反应条件
1.1: 98 percent / H2 / Rh/C / tetrahydrofuran / 18 h / 76000 Torr 2.1: 90 percent / pyridinium chlorochromate; Celite; sodium carbonate / CH2Cl2 / 4 h / 20 °C 3.1: 90 percent / p-toluenesulfonic acid monohydrate / toluene / 18 h / Heating 4.1: 95 percent / LiAlH4 / diethyl ether / 3 h / 20 °C 5.1: 97 percent / oxalyl chloride; DMSO; triethylamine / CH2Cl2 / 2 h / -60 - 20 °C 6.1: sodium cyanide / ethanol / 2 h 6.2: 75 percent / NH3 / ethanol / 16 h / 90 - 110 °C 7.1: 94 percent / HCl / 1 h / 20 °C View Scheme
参考文献
Kitbunnadaj, Ruengwit; Hoffmann, Marcel; Fratantoni, Silvina A.; Bongers, Gerold; Bakker, Remko A.; Wieland, Kerstin; El Jilali, Ahmed; De Esch, Iwan J. P.; Menge, Wiro M. P. B.; Timmerman, Henk; Leurs, Rob
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 23 p. 6309 - 6323
