1: formyl formic acid With acetic anhydride; ytterbium(III) triflate T=20°C; 0.166667 h; 2: para-bromoacetophenone With acetic acid in acetic acid T=140°C; 0.5 h; Microwave irradiationSealed tube;
参考文献
Tolstoluzhsky, Nikita; Nikolaienko, Pavlo; Gorobets, Nikolay; Van Der Eycken, Erik V.; Kolos, Nadezhda
European Journal of Organic Chemistry, 2013 , # 24 p. 5364 - 5369
1: With 10 palladium on activated charcoal; potassium carbonate in toluene T=115°C; Suzuki-Miyaura reaction; 24 h; Inert atmospheresolid phase reaction; 2: With water; potassium hydroxide in ethanol T=90°C; 72 h; 3: With hydrogenchloride in ethanol; dichloromethane; water
参考文献
Gruber-Woelfler; Radaschitz; Feenstra; Haas; Khinast
Journal of Catalysis, 2012 , vol. 286, p. 30 - 40
