1.1: Mg / diethyl ether
1.2: diethyl ether / 1.5 h / Heating
2.1: aq. sulfuric acid / diethyl ether / 1 h / Heating
2.2: 7.70 g / p-toluenesulfonic acid / toluene / 3 h / Heating
3.1: 2.18 g / dimethylformamide / 20 h / Heating
View Scheme
参考文献
Van Walree, Cornelis A.; Kaats-Richters, Veronica E. M.; Veen, Sandra J.; Wieczorek, Birgit; Van Der Wiel, Johanna H.; Van Der Wiel, Bas C.
European Journal of Organic Chemistry, 2004 , # 14 p. 3046 - 3056
Okamoto, Tsuyoshi; Kakinami, Takaaki; Nishimura, Tetsuo; Irwan-Hermawan; Kajigaeshi, Shoji
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 6 p. 1731 - 1733
naphthalene; manganese(II) halide; lithium in tetrahydrofuran
Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rieke, Reuben D.; Kim, Seung-Hoi
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 5235 - 5239