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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-溴苯乙酮
合成路线
（共 1006 条）
99-90-1
4-溴苯乙酮
→
反应条件
89671-78-3
反应条件
1: 75 percent / KOH / ethanol / 3 h / 20 °C 2: 75 percent / methanol / 1.5 h / Irradiation View Scheme
参考文献
Kar, Samiran; Lahiri, Saswati
Journal of the Indian Chemical Society, 1999 , vol. 76, # 11-12 p. 607 - 610
99-90-1
4-溴苯乙酮
→
反应条件
90162-44-0
甲基苯甲醇-D4
+
116772-84-0
反应条件
NaOD; copper aluminide T=50°C; 2.33333 h; addition gradually; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tashiro, Masashi; Mataka, Shuntaro; Nakamura, Hiroshi; Nakayama, Kouji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 179 - 182
99-90-1
4-溴苯乙酮
+
59020-10-9
3-(三正丁基锡)吡啶
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
copper(l) iodide; C37H51ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide T=80°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
99-90-1
4-溴苯乙酮
+
1692-25-7
吡啶-3-硼酸
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
potassium phosphate; palladium dichloride; S-2,2',6,6'-tetramethoxy-4,4'-bis(diphenylphosphino)-3,3'-bipyridine in butan-1-ol T=100°C; Suzuki coupling; 20 h; Inert atmosphere;
参考文献
Fu, Xing-Li; Wu, Lei-Lei; Fu, Hai-Yan; Chen, Hua; Li, Rui-Xiang
European Journal of Organic Chemistry, 2009 , # 13 p. 2051 - 2054
1120-90-7
+
99-90-1
4-溴苯乙酮
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
1: para-bromoacetophenone With indium; bathophenanthroline; 3-chloroprop-1-ene; lithium chloride; cobalt(II) dibromide in tetrahydrofuran T=100°C; 15 h; Inert atmosphere; 2: 3-iodo-pyridine With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=80°C; 18 h; Inert atmosphere;
参考文献
Adak, Laksmikanta; Yoshikai, Naohiko
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7563 - 7568
99-90-1
4-溴苯乙酮
+
160688-99-3
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in 1,4-dioxane Suzuki cross-coupling reaction; 16 h; Heating;
参考文献
Cioffi, Christopher L.; Spencer, William T.; Richards, Justin J.; Herr, R. Jason
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2210 - 2212
99-90-1
4-溴苯乙酮
+
329214-79-1
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 6 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
99-90-1
4-溴苯乙酮
+
89878-14-8
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
potassium hydroxide; tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide in tetrahydrofuran 2 h; Heating;
参考文献
Ishikura, Minoru; Kamada, Machiko; Terashima, Masanao
Heterocycles, 1984 , vol. 22, # 2 p. 265 - 268
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
copper(l) iodide; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=80°C; 22 h; Inert atmosphere;
参考文献
Yamamoto, Yasunori; Takizawa, Miho; Yu, Xiao-Qiang; Miyaura, Norio
Heterocycles, 2010 , vol. 80, # 1 p. 359 - 368
61-54-1
+
99-90-1
4-溴苯乙酮
→
反应条件
906067-45-6
反应条件
dihydrogen peroxide; iodine in water; dimethyl sulfoxide T=110°C;
参考文献
Zhu, Yan-Ping; Liu, Mei-Cai; Cai, Qun; Jia, Feng-Cheng; Wu, An-Xin
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10132 - 10137
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