您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-溴苯乙酮
合成路线
（共 1006 条）
201230-82-2
+
99-90-1
4-溴苯乙酮
+
98-80-6
苯硼酸
→
反应条件
53689-84-2
反应条件
C57H43IP2Pd; potassium carbonate in 1,4-dioxane T=130°C; carbonylative Suzuki coupling; P=3750.38 Torr; 24 h; Autoclave;
参考文献
Kaganovsky, Luba; Gelman, Dmitri; Rueck-Braun, Karola
Journal of Organometallic Chemistry, 2010 , vol. 695, # 2 p. 260 - 266
4406-73-9
+
99-90-1
4-溴苯乙酮
+
82102-37-2
→
反应条件
53689-84-2
反应条件
bis(acetylacetonato) palladium; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4; cataCXium® AHI in water; N,N-dimethyl-formamide; toluene T=80°C; Suzuki-Miyaura Coupling; 16 h; Inert atmosphereGlovebox;
参考文献
Bjerglund, Klaus M.; Skrydstrup, Troels; Molander, Gary A.
Organic Letters, 2014 , vol. 16, # 7 p. 1888 - 1891
→
反应条件
53689-84-2
反应条件
bis(acetylacetonato) palladium; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4; cataCXium® AHI in toluene T=80°C; Suzuki-Miyaura Coupling; 16 h; Reagent/catalyst;
参考文献
Bjerglund, Klaus M.; Skrydstrup, Troels; Molander, Gary A.
Organic Letters, 2014 , vol. 16, # 7 p. 1888 - 1891
→
反应条件
92-91-1
+
53689-84-2
反应条件
bis(acetylacetonato) palladium; tris(isopropyl)phosphonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in toluene T=80°C; Suzuki-Miyaura Coupling; 16 h; Reagent/catalyst;
参考文献
Bjerglund, Klaus M.; Skrydstrup, Troels; Molander, Gary A.
Organic Letters, 2014 , vol. 16, # 7 p. 1888 - 1891
960-16-7
+
99-90-1
4-溴苯乙酮
+
13939-06-5
→
反应条件
53689-84-2
反应条件
palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] dichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride in N,N-dimethyl-formamide T=100°C; Stille carbonylative cross-coupling; 16 h;
参考文献
Lindh, Jonas; Fardost, Ashkan; Almeida, Maria; Nilsson, Peter
Tetrahedron Letters, 2010 , vol. 51, # 18 p. 2470 - 2472
201230-82-2
+
99-90-1
4-溴苯乙酮
+
98-80-6
苯硼酸
→
反应条件
92-91-1
+
53689-84-2
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; potassium iodide in various solvent(s) T=80°C; P=760 Torr; 16 h; further reagents;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
99-90-1
4-溴苯乙酮
+
100-52-7
→
反应条件
53689-84-2
+
94705-09-6
反应条件
[2,2']bipyridinyl; Fe/Cr/Ni in N,N-dimethyl-formamide Nozaki-Hiyama-Kishi reaction; Electrolysis;
参考文献
Durandetti; Nedelec; Perichon
Organic letters, 2001 , vol. 3, # 13 p. 2073 - 2076
99-90-1
4-溴苯乙酮
+
98-80-6
苯硼酸
→
反应条件
92-91-1
+
53689-84-2
反应条件
bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; potassium carbonate in various solvent(s) T=80°C; 16 h; further reagents;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
99-90-1
4-溴苯乙酮
→
反应条件
5467-56-1
反应条件
1.1: copper(l) iodide; 8-Hydroxyquinoline 1-oxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere 1.2: 24 h / 110 °C / Inert atmosphere 2.1: cesium hydroxide monohydrate; tetra-(n-butyl)ammonium iodide / water; dimethyl sulfoxide / 12 h / 100 °C / Inert atmosphere View Scheme
参考文献
Yang, Kai; Li, Zheng; Wang, Zhaoyang; Yao, Zhiyi; Jiang, Sheng
Organic Letters, 2011 , vol. 13, # 16 p. 4340 - 4343
99-90-1
4-溴苯乙酮
→
反应条件
55368-74-6
反应条件
1: NaOMe, MeOH 2: aq. NH2OH*HCl, NaOH / dioxane / 24 h / Heating View Scheme
参考文献
Dann,O. et al.
Justus Liebigs Annalen der Chemie, 1975 , p. 160 - 194
首页
上一页
1
...
86
87
88
89
90
91
92
...
101
下一页
末页
到第
页
确定
