反应条件
lithium aluminium tetrahydride; n-butyllithium 1) THF, -78 deg C, 1 h, 2) THF, -78 deg C -> -5 deg C, 30 min, 3) THF, -5 deg C -> room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 27, # 19 p. 3333 - 3339
