tetrachlorosilane; zinc(II) chloride in dichloromethane
T=20°C; 18 h;
参考文献
Badawy, Doria S.; Abdel-Galil, Ebrahim; Kandeel, Ezzat M.; Basyouni, Wahid M.; Khatab, Tamer K.
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 11 p. 2799 - 2812
tetrachlorosilane; zinc(II) chloride in dichloromethane
T=20°C; 19 h;
参考文献
Badawy, Doria S.; Abdel-Galil, Ebrahim; Kandeel, Ezzat M.; Basyouni, Wahid M.; Khatab, Tamer K.
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 11 p. 2799 - 2812
1: 2-methylphenylmagnesium chloride With zinc(II) chloride in tetrahydrofuran
T=20°C; 0.333333 h;
2: para-chloroacetophenone With Pd0(tris(tert-butyl)phosphine)2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=100°C; Negishi reaction; 2 h; Further stages.;
参考文献
Dai; Fu
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2719 - 2724
