1: With sodium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); 2-(dicyclohexylphosphino)-2'-methylbiphenyl in ethanol; water T=78 - 80°C; Suzuki coupling; Inert atmosphere; 2: With hydrogenchloride; water in ethanol T=20°C; pH=3.4; Inert atmosphere;
参考文献
Achmatowicz, Michal; Thiel, Oliver R.; Wheeler, Philip; Bernard, Charles; Huang, Jinkun; Larsen, Robert D.; Faul, Margaret M.
Journal of Organic Chemistry, 2009 , vol. 74, # 2 p. 795 - 809
1: With copper(l) iodide; caesium carbonate; L-proline in dimethyl sulfoxide T=130°C; Ullmann type reaction; 24 h; Inert atmosphere; 2: in dimethyl sulfoxide T=140°C; 12 h; 3: With hydrogenchloride in water pH=2 - 3;
参考文献
Yang, Daoshan; Yang, Haijun; Fu, Hua
Chemical Communications, 2011 , vol. 47, # 8 p. 2348 - 2350
