N,N-二甲基-对苯二胺合成路线 (共 293 条)
参考文献
Chemische Berichte, , vol. 18, p. 575
Journal of the American Chemical Society, , vol. 30, p. 399,400, 401
反应条件
TEA in dichloromethane T=0 - 25°C; Acylation; 3 h;
参考文献
Patel, Mona; Ko, Soo S.; McHugh Jr., Robert J.; Markwalder, Jay A.; Srivastava, Anurag S.; Cordova, Beverly C.; Klabe, Ronald M.; Erickson-Viitanen, Susan; Trainor, George L.; Seitz, Steven P.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 19 p. 2805 - 2810
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; potassium carbonate in toluene T=110°C; 6 h; Inert atmosphere;
参考文献
Fristrup, Peter; Tursky, Matyas; Madsen, Robert
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2569 - 2577
反应条件
triethylamine in tetrahydrofuran T=25°C; 12 h;
参考文献
Wilcox, Craig S.; Kim, Eun-il; Romano, David; Kuo, Lung Huang; Burt, Arthur L.; Curran, Dennis P.
Tetrahedron, 1995 , vol. 51, # 2 p. 621 - 634
反应条件
sodium hydroxide in dichloromethane T=0 - 20°C; 21 h;
参考文献
Li, Zheng-Yi; Ma, Hong-Zhao; Han, Chen; Xi, Hai-Tao; Meng, Qi; Chen, Xin; Sun, Xiao-Qiang
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-F0228-OP, p. 1667 - 1674
反应条件
1: With triethylamine in methanol T=0 - 5°C; 2: With bis(trichloromethyl) carbonate in chloroform T=0°C; 4 h; Further stages.;
参考文献
Chaskar; Yewale; Bhagat; Langi
Synthetic Communications, 2008 , vol. 38, # 12 p. 1972 - 1975
参考文献
Peck et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2364
反应条件
1: NH3 / 0.5 h 2: lead sulfide / H2O / Heating View Scheme
参考文献
Li, Zheng-Yi; Ma, Hong-Zhao; Han, Chen; Xi, Hai-Tao; Meng, Qi; Chen, Xin; Sun, Xiao-Qiang
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-F0228-OP, p. 1667 - 1674
反应条件
in dichloromethane T=20°C; 2 h;
参考文献
Mittapalli, Gopi Kumar; Vellucci, Danielle; Yang, Jun; Toussaint, Marion; Brothers, Shaun P.; Wahlestedt, Claes; Roberts, Edward
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 12 p. 3916 - 3920
参考文献
Zetzsche; Fredrich
Chemische Berichte, 1940 , vol. 73, p. 1420,1422,1423