N,N-二甲基-对苯二胺合成路线 （共 293 条）
参考文献
Zetzsche; Fredrich
Chemische Berichte, 1940 , vol. 73, p. 1420,1422,1423
反应条件
Ag/C; potassium hydroxide in dimethyl sulfoxide T=60°C; P=760.051 Torr; 30 h; Green chemistry; Catalytic behavior;
参考文献
Cai, Shuangfei; Rong, Hongpan; Yu, Xiaofei; Liu, Xiangwen; Wang, Dingsheng; He, Wei; Li, Yadong
ACS Catalysis, 2013 , vol. 3, # 4 p. 478 - 486
反应条件
pyridine in N,N-dimethyl-formamide T=0 - 20°C; 1 h;
参考文献
AVENTIS PHARMA S.A.
Patent: WO2006/10643 A1, 2006 ;
Location in patent: Page/Page column 73-74 ;
WO 2006/010643 A1
反应条件
triethylamine in toluene
参考文献
Doub et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 2205,2210
反应条件
carbon in ethyl acetate Heating;
参考文献
Stark, Holger; Purand, Katja; Ligneau, Xavier; Rouleau, Agnes; Arrang, Jean-Michel; Garbarg, Monique; Schwartz, Jean-Charles; Schunack, Walter
Journal of Medicinal Chemistry, 1996 , vol. 39, # 5 p. 1157 - 1163
反应条件
1: 4-(dimethylamino)aniline With hydrogenchloride; sodium nitrite in water Cooling with ice; 2: phenol With sodium hydroxide in water T=5°C;
参考文献
Cui, Kun; Lu, Xuemin; Cui, Wei; Wu, Jun; Chen, Xumeng; Lu, Qinghua
Chemical Communications, 2011 , vol. 47, # 3 p. 920 - 922
参考文献
Wong, Wai-Yeung; Wong, Wing-Tak
Journal of Organometallic Chemistry, 1999 , vol. 584, # 1 p. 48 - 57
反应条件
1: CHCl3 / 2 h
2: aq. HCl / ethanol / 3 h / Heating
3: 59.9 percent / aq. ammonia
View Scheme
参考文献
Ryczek, Jozef
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 5 p. 997 - 1000
反应条件
1: durch Austausch von NH2 gegen Chlor nach Sandmeyer
2: hydrochloric acid; NaNO2
View Scheme
参考文献
Heidlberg
Chemische Berichte, 1887 , vol. 20, p. 150
反应条件
1: 130 °C
2: nitrobenzene
View Scheme
参考文献
Gertschuk
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 731,736
Chem.Abstr., 1942 , p. 218
