2-溴-7-己基-9H-芴合成路线 （共 4 条）
反应条件
bromine in chloroform
1.) RT; 3 h, 2.) reflux, 2 h,;
参考文献
Davison, I. R.; Hall, D. Muriel; Sage, I.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 129, p. 17 - 36
反应条件
1: hydrazine hydrate; potassium hydroxide / bis-(2-hydroxy-ethyl) ether / Heating
2: bromine / CHCl3 / Heating
View Scheme
参考文献
Boardman, Frederick H.; Dunmur, David A.; Grossel, Martin C.; Luckhurst, Geoffrey R.
Chemistry Letters, 2002 , # 1 p. 60 - 61
反应条件
1: aluminum chloride / 1,1,2,2-tetrachloro-ethane / 0 °C
2: hydrazine hydrate; potassium hydroxide / bis-(2-hydroxy-ethyl) ether / Heating
3: bromine / CHCl3 / Heating
View Scheme
参考文献
Boardman, Frederick H.; Dunmur, David A.; Grossel, Martin C.; Luckhurst, Geoffrey R.
Chemistry Letters, 2002 , # 1 p. 60 - 61
反应条件
1: aluminum chloride / 1,1,2,2-tetrachloro-ethane / 0 °C
2: hydrazine hydrate; potassium hydroxide / bis-(2-hydroxy-ethyl) ether / Heating
3: bromine / CHCl3 / Heating
View Scheme
参考文献
Boardman, Frederick H.; Dunmur, David A.; Grossel, Martin C.; Luckhurst, Geoffrey R.
Chemistry Letters, 2002 , # 1 p. 60 - 61
