N,N-二甲基-1H-吲唑-3-羧酰胺合成路线 （共 5 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 0.5 h; 2: With Glauber's salt in tetrahydrofuran 1 h;
参考文献
KYOWA HAKKO KOGYO CO., LTD.
Patent: EP1650194 A1, 2006 ;
Location in patent: Page/Page column 24 ;
反应条件
1: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in tetrahydrofuran
T=20°C;
2: With sodium hydrogencarbonate in water; ethyl acetate
参考文献
KYOWA HAKKO KOGYO CO., LTD.
Patent: EP1650194 A1, 2006 ;
Location in patent: Page/Page column 24 ;
参考文献
Snyder et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 2009,2010
反应条件
1: SOCl2
2: H2O
View Scheme
参考文献
Smith; Kirchner
Journal of Organic Chemistry, 1958 , vol. 23, p. 621
参考文献
Smith; Kirchner
Journal of Organic Chemistry, 1958 , vol. 23, p. 621
