反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1: sodium hydroxide / 2 h / 0 - 20 °C / |Inert atmosphere<br />2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere<br />3: ammonium hydroxide / 0 - 20 °C / |Inert atmosphere<br />4: FeSO<sub>4</sub>.(NH<sub>4</sub>)<sub>2</sub>SO<sub>4</sub>.6H<sub>2</sub>O; isopropyl 1-thio-β-D-galactopyranoside / aq. phosphate buffer / 48 h / 37 °C<br /> <br />
参考文献
Sirasani, Gopal; Tong, Liuchuan; Balskus, Emily P. Angewandte Chemie - International Edition, 2014 , vol. 53, # 30 p. 7785 - 7788 Angew. Chem., 2014 , vol. 53, # 30 p. 7919 - 7922,4
