1: triethylamine / dichloromethane / 12 h / 20 °C 2: water; methanol / |UV-irradiation; |Photolysis View Scheme

1: triethylamine / dichloromethane / 12 h / 20 °C 2: water; methanol / |UV-irradiation; |Photolysis View Scheme

暂无反应条件数据

暂无反应条件数据

1: 1) n-BuLi / 1) tetrahydrofuran, hexane, -78 deg C, 30 min, 2) tetrahydrofuran, 1h 2: 1) lithium diisopropylamide / 1) tetrahydrofuran, hexane, -78 deg C, 1h, 2) tetrahydrofuran, 5h, -78 up to 0 deg C 3: H2 / 10percent Pd-C / ethanol / Ambient temperature 4: 97 percent / DEPC, triethylamine / tetrahydrofuran / 2 h / 0 °C 5: 83 percent / LiOH*H2O / tetrahydrofuran; H2O / 3 h / 0 °C 6: 71 percent / DEPC, triethylamine / tetrahydrofuran / 8 h / 0 °C View Scheme

1: triethylamine / dichloromethane / 12 h / 20 °C 2: water; methanol / |UV-irradiation; |Photolysis View Scheme