4-甲氧基-1,3-苯二酚3-乙酸酯合成路线 （共 8 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 2.5 h; Heating;
参考文献
Aihara, Kazuhiro; Urano, Yasuteru; Higuchi, Tsunehiko; Hirobe, Masaaki
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2165 - 2170
反应条件
1: 3-hydroxy-4-methoxy-benzaldehyde; acetic anhydride 2: With 3-chloro-benzenecarboperoxoic acid in dichloromethane 3: With sodium hydrogencarbonate in ethanol
参考文献
Tetrahedron, , vol. 60, # 52 p. 12211 - 12216
反应条件
1: 95 percent / DMAP, Et3N / tetrahydrofuran; diethyl ether / 14 h / Ambient temperature 2: 87.5 percent / m-chloroperbenzoic acid / CH2Cl2 / 2.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 11 p. 2165 - 2170
参考文献
Aihara, Kazuhiro; Urano, Yasuteru; Higuchi, Tsunehiko; Hirobe, Masaaki
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2165 - 2170
反应条件
1: Cs2CO3 / dimethylformamide / 5 h / Ambient temperature 2: 25percent aq. NH3 / dimethylformamide / 0.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 11 p. 2165 - 2170
反应条件
ammonium hydroxide in methanol 2 h; Ambient temperature;
参考文献
Aihara, Kazuhiro; Urano, Yasuteru; Higuchi, Tsunehiko; Hirobe, Masaaki
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2165 - 2170
反应条件
boron trifluoride diethyl etherate
T=70°C; Fries rearrangement;
参考文献
Hayakawa, Ichiro; Shioda, Shuya; Ikedo, Akiyuki; Kigoshi, Hideo
Bulletin of the Chemical Society of Japan, 2014 , vol. 87, # 4 p. 544 - 549
参考文献
THE UNIVERSITY COURT OF THE UNIVERSITY OF ST ANDREWS
Patent: WO2004/69774 A2, 2004 ;
Location in patent: Page 89 ;
