(2-苯基乙基)硫代]乙酸合成路线 (共 10 条)
反应条件
1: 75 percent / 30percent H2O2 / acetic acid / 2 h / Heating 2: 60 percent / benzylamine, glacial acetic acid / 3 h 3: 72 percent / 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ) / dioxane / 8 h / Heating 4: 78 percent / dichlorotris(triphenylphosphine)ruthenium(II), HCl gas / benzene / Heating View Scheme
参考文献
Ramana Reddy; Manjubhashini; Reddy; Bhaskar Reddy
Synthetic Communications, 1991 , vol. 21, # 15-16 p. 1589 - 1596
反应条件
1: 75 percent / 30percent H2O2 / acetic acid / 2 h / Heating 2: 60 percent / benzylamine, glacial acetic acid / 3 h 3: 72 percent / 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ) / dioxane / 8 h / Heating 4: 78 percent / dichlorotris(triphenylphosphine)ruthenium(II), HCl gas / benzene / Heating View Scheme
参考文献
Ramana Reddy; Manjubhashini; Reddy; Bhaskar Reddy
Synthetic Communications, 1991 , vol. 21, # 15-16 p. 1589 - 1596
反应条件
sulfuric acid; mercuric sulphate
参考文献
Holmberg
Arkiv foer Kemi, 1938 , vol. 12 A, # 28 p. 4
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 141, p. 93,106
参考文献
Holmberg
Arkiv foer Kemi, 1938 , vol. 12 A, # 28 p. 4
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 141, p. 93,106
反应条件
sodium hydroxide in methanol
5 h; Heating;
参考文献
Ramana Reddy; Manjubhashini; Reddy; Bhaskar Reddy
Synthetic Communications, 1991 , vol. 21, # 15-16 p. 1589 - 1596
反应条件
sodium hydroxide in methanol
T=20°C;
参考文献
Ning, Xianling; Guo, Ying; Wang, Xiaowei; Ma, Xiaoyan; Tian, Chao; Shi, Xueqi; Zhu, Renzong; Cheng, Can; Du, Yansheng; Ma, Zhizhong; Zhang, Zhili; Liu, Junyi
Journal of Medicinal Chemistry, 2014 , vol. 57, # 10 p. 4302 - 4312
参考文献
Angehrn, Peter; Hunziker, Daniel; Wyss, Pierre-Charles
Patent: US2003/199459 A1, 2003 ;
参考文献
v. Braun; Weissbach
Chemische Berichte, 1929 , vol. 62, p. 2420
参考文献
Holmberg
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 141, p. 93,96
Arkiv foer Kemi, 1937 , vol. 12 A, # 14 p. 3,4
参考文献
Kharasch; May; Mayo
Journal of Organic Chemistry, 1938 , vol. 3, p. 186