反应条件
in hexane
combining (Me3Si)PhPH soln. with (Me3Si)Al.Et2O soln. at -78 °C, warming to 25 °C, stirring 4 h, evapn. of solvent, redissolution of resulting oil in hexane, refluxing for 48 h ; under inert gas; concn., decantation, washing of residue with cold hexane (improvement of yield by collection of decanted liquids and filtrates and crystn. from hexane at -20 °C), drying in vacuo;
参考文献
Janik, Jerzy F.; Duesler, Eileen N.; McNamara, William F.; Westerhausen, Matthius; Paine, Robert T.
Organometallics, 1989 , vol. 8, p. 506 - 514
