反应条件
in ethylene glycol dimethyl ether; pentane LiGeMe3 in pentane is dropped slowly to a soln. of Sm complex in DME; reaction for 4 h at room temp.; decantation, concn., cooling to -78°C; pptn. of bis(tris(cyclopentadienyl)samarium complex the next day, (Cp2SmCl)2 crystallizes from the decanted soln.; elem. anal.;
参考文献
Schumann, Herbert; Nickel, Siegbert; Loebel, Joerg; Pickardt, Joachim
Organometallics, 1988 , vol. 7, p. 2004 - 2009
