in tetrahydrofuran
addn. of Sn-compound in soln. to Ti-compound in hexane (-78°C), stirred, temp. raised to 0°C; solvent evapd. in vac., residue washed with pentane and dried; GLC;
参考文献
Vyshinskaya, L. I.; Timoshenko, S. Ya.; Vishnyakova, T. A.
Journal of General Chemistry USSR (English Translation), 1990 , vol. 60, p. 1729 - 1733
Zhurnal Obshchei Khimii, 1990 , vol. 60, p. 1937 - 1942
in ammonia
NH3 (liquid); molar ratio acetylene/Sn-compd. 2/1, 20°C; elem. anal.;
参考文献
Zavgorodnii, V. S.; Zubova, T. P.; Simin, V. B.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 1765 - 1773
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 2048 - 2057
azodiisobutyric acid dinitrile in not given
byproducts: C6H5OH;
参考文献
Creemers, H. M. J. C.; Noltes, J. G.
Rec. Trav. Chim., 1965 , vol. 84, p. 1589 - 1593
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.5, page 34 - 36
in ammonia
NH3 (liquid); molar ratio acetylene/Sn-compd. 2/1, -34°C; elem. anal.;
参考文献
Zavgorodnii, V. S.; Zubova, T. P.; Simin, V. B.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 1765 - 1773
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 2048 - 2057
in tetrahydrofuran
molar ratio acetylene/Sn-compd. 2/1, 20°C; elem. anal.;
参考文献
Zavgorodnii, V. S.; Zubova, T. P.; Simin, V. B.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 1765 - 1773
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 2048 - 2057
azodiisobutyric acid dinitrile in further solvent(s)
byproducts: C6H6, (C2H5)(CH3)NH, CH4; reaction for 6 h at 80°C in cumol in presence of azoisobutyric acid dinitrile;;
参考文献
Hollaender, J.; Neumann, W. P.
Angewandte Chemie, 1971 , vol. 83, p. 850 - 851
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.2, page 22 - 31
