2-苯基噻唑烷-4-羧酸甲酯合成路线 (共 3 条)
反应条件
1: 48 percent / N-bromosuccinamide; benzoyl peroxide / CCl4 / 6 h / Heating 2: aq. NaOH; EtOAc / methanol / 2 h / 0 °C View Scheme
参考文献
Gududuru, Veeresa; Hurh, Eunju; Dalton, James T.; Miller, Duane D.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 7 p. 2584 - 2588
反应条件
sodium hydrogencarbonate in ethanol; water
3 h;
参考文献
UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION; OHIO STATE UNIVERSITY RESEARCH FOUNDATION
Patent: WO2005/49591 A1, 2005 ;
Location in patent: Page/Page column 27-28 ;
反应条件
N-Bromosuccinamide; dibenzoyl peroxide in tetrachloromethane
6 h; Heating;
参考文献
Gududuru, Veeresa; Hurh, Eunju; Dalton, James T.; Miller, Duane D.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 7 p. 2584 - 2588